At the end of a reaction it is important to remove the solvent from a solid product (more than one answer may be correct):

a. So that the melting point can be determined.
b. So that clean NMR spectra can be obtained that do not contain solvent peaks.
c. So that the yield can be determined.
d. So that the solvent can be reused.

Answers

Answer 1

Answer:

(B.) and (C.)

b. So that clean NMR spectra can be obtained that do not contain solvent peaks.

c. So that the yield can be determined.

Explanation:

The solvent used in Nuclear Magnetic Resonance (NMR) spectrometer is Trimethyl silane (TMS), a neutral solvent which doesn't give off any signals. Other solvents could have interactions with the radiation, and disrupt the spectra.

Furthermore, for accurate determination of the actual yield and overall percentage yield, solid must be separated from the solvent, dried and weighed.

I hope this was explanatory enough.


Related Questions

why are the products of light reaction of photosythesis important

Answers

Answer: light reaction produces oxygen and water as we know the general importance of oxygen and water they are useful for organism to survive if plants do not produce oxygen then how could we get oxygen from the environment

How to treat stream water for drinking

Answers

Answer:

Explanation:

Boiling.

Use water filter

Use Ultraviolet Light.

Use chlorine drops

I would recomade boiling as the main

because its the easiest and cheapest Or water filter if you have one

Consider the following reaction where Kc = 1.29×10-2 at 600 K: COCl2 (g) CO (g) + Cl2 (g) A reaction mixture was found to contain 0.104 moles of COCl2 (g), 4.66×10-2 moles of CO (g), and 3.76×10-2 moles of Cl2 (g), in a 1.00 liter container. Indicate True (T) or False (F) for each of the following:
1. In order to reach equilibrium COCl2(g) must be consumed.
A. True B. False
2. In order to reach equilibrium Kc must increase.
A. True B. False
3. In order to reach equilibrium CO must be consumed.
A. True B. False
4. Qc is greater than Kc.
A. True B. False
5. The reaction is at equilibrium. No further reaction will occur.
A. True B. False

Answers

Answer:

1. In order to reach equilibrium COCl₂(g) must be consumed.

B. False

2. In order to reach equilibrium Kc must increase.

B. False .

3. In order to reach equilibrium CO must be consumed.

A. True.

4. Qc is greater than Kc.

A. True

5. The reaction is at equilibrium. No further reaction will occur.

B. False.

Explanation:

Based on the reaction:

COCl₂(g) → CO (g) + Cl₂(g)

And Kc is defined as:

Kc = 1.29x10⁻² = [CO] [Cl₂] / [COCl₂]

Molar concentrations of each species are:

[COCl₂] = 0.104 moles of COCl₂ / 1L = 0.104M

[CO] = 4.66×10⁻² moles of CO / 1L = 4.66×10⁻²M

[Cl₂] = 3.76×10⁻² moles of Cl₂ / 1L = 3.76×10⁻²M

Replacing in Kc formula:

4.66×10⁻²M × 3.76×10⁻²M / 0.104M = 1.68x10⁻²

As the concentrations are not in equilibrium, 1.68x10⁻² is defined as the reaction quotient, Qc.

As Qc > Kc, the reaction will shift to the left producing more COCl₂ and consuming CO and Cl₂. Thus

1. In order to reach equilibrium COCl₂(g) must be consumed.

B. False

2. In order to reach equilibrium Kc must increase.

B. False . Kc is a constant that never change.

3. In order to reach equilibrium CO must be consumed.

A. True.

4. Qc is greater than Kc.

A. True

5. The reaction is at equilibrium. No further reaction will occur.

B. False. The reaction is in equilibrium when Qc = Kc

A pure sample of the R enantiomer of a compound has a specific rotation, [ α], of +20 °. A solution containing 0.2 g/mL of a mixture of enantiomers rotates plane polarized light by −2 ° in a 1 dm polarimeter. What is the enantiomeric excess (%ee) of the mixture?

Answers

Answer:

Explanation:

The specific rotation of the sample is -2 degrees/0.2 g/mL of mixture

This equals -10 degrees/g/mL of sample.

let the proportion of the R (+) enantiomer be x. The proportion of the S (-) enantiomer in the mixture will be given by (1-x).

specific rotation of the mixture = proportion of R enantiomer* its specific rotation + proportion of S enantiome * its specific rotation

i.e.

-10 = x *(+20) + (1-x)*(-20)

-10 = 20x-20 + 20x

-10+20 = 40x

+10 = 40 x

x=10/40 = 25%

Since the proportion of the other enantiomer is 1-x, it is 0.75 or 75%

So the mixture contains 25% R, 75% S, giving you an excess of 50%.

Answer:

10%

Explanation:

Enantiomeric excess is a way of describing how optically pure a mixture is by calculating the purity of the major enantiomer. It can range from 0%-100%. Enantiomeric excess ( ee ) can also be defined as the absolute difference between the mole fractions of two enantiomers.

Enantiomeric excess is also called optical purity. This is because chiral molecules cause the rotation of plane-polarized light and are said to be optically active. An enantiomerically pure sample has an enantiomeric excess of 100 percent

Enantiomeric excess = observed specific rotation/specific rotation of the pure enantiomer x 100

From the data given in the question;

observed specific rotation= -2°

specific rotation of the pure enantiomer = +20°

Therefore;

ee= 2/20 ×100

ee= 10%

When a saturated solution of NH4Br dissolved in 100 grams of water is cooled from 60°C to 30°C, how much NH4Br will precipitate?

Answers

Answer:

[tex]m_{precipitated}=24.8g[/tex]

Explanation:

Hello,

In this case, since at 60 °C, 108 grams of ammonium bromide are completely dissolved in 100 grams of water for a saturated solution, once it is cooled to 30 °C, wherein only 83.2 grams are completely dissolved in 100 grams of water, the following mass will precipitate:

[tex]m_{precipitated}=108g-83.2g\\\\m_{precipitated}=24.8g[/tex]

Best regards.

A student dissolved 5.00 g of Co(NO3)2 in enough water to make 100. mL of stock solution. He took 4.00 mL of the stock solution and then diluted it with water to give 275. mL of a final solution. How many grams of NO3- ion are there in the final solution?

Answers

Answer:

0.136g

Explanation:

A student dissolved 5.00 g of Co(NO3)2 in enough water to make 100. mL of stock solution. He took 4.00 mL of the stock solution and then diluted it with water to give 275. mL of a final solution. How many grams of NO3- ion are there in the final solution?

[tex]Co(NO_3)_2(aq)\rightarrow Co^{2+}(aq)+2NO_3^{-}(aq)[/tex]

Initial mole of Co(NO3)2  [tex]=\frac{mass}{molar mass}[/tex]

[tex]=\frac{5.00}{182.94} \\\\=0.02733mol[/tex]

Mole of Co(NO3)2 in final solution

[tex]=\frac{4.00}{100}\times 0.02733\\\\=0.04\times 0.02733\\\\= 0.001093mol[/tex]

Mole of  NO3- in final solution = 2 x Mole of Co(NO3)2

[tex]=2\times 0.001093\\\\=0.002186mol[/tex]

Mass of  NO3- in final solution is mole x Molar mass of NO3

[tex]=0.002186\times62.01\\\\=0.136g[/tex]

The final solution contains 0.24 g of nitrate ion.

Number of moles of  Co(NO3)2 =  5.00 g/183 g/mol = 0.027 moles

Number of moles = concentration × volume

concentration = Number of moles /volume

Volume of solution = 100 mL or 0.1 L

concentration =  0.027 moles/0.1 L = 0.27 M

Using the dilution formula;

C1V1 = C2V2

C1 =  0.27 M

V1 = 4.00 mL

C2 = ?

V2 =  275. mL

C2 = C1V1/V2

C2 = 0.27 × 4.00/ 275

C2 = 0.0039 M

Number of moles of NO3- ion in Co(NO3)2 = 0.0039 M × 62 g/mol = 0.24 g

Learn more: https://brainly.com/question/1340582

In this lab, you are to carry out the formation of a Grignard reagent from 1-bromo-benzene andits subsequent reaction with solid carbon dioxide (CO2) followed by acidic workup (using HCl asthe acid). Write the overall reaction and product(s) that you expect.

Answers

Answer:

(A). C6H5Br + Mg(in ether) -----------> C6H5MgBr.

(B). C6H5MgBr + O = C = O -----------> C6H5-COO^- Mg^+ Br.

(C). C6H5-COO^- Mg^+ Br + HCl --------> C6H5-COOH + Mg^+Br(OH).

PRODUCTS=> C6H5-COOH and Mg^+Br(OH).

Explanation:

A Grignard reagent is a reagent that/which is an organometallic compound that is R -Mg- X. The R = alkyl, vinyl or allyl and the X = halogens.

It must be noted that an important reaction of Grignard reagent is its reaction with compounds containing the Carbonyl that is -CO functional group and this kind of Reaction is known as a Grignard Reaction.

So, in this question we are told that;

=> "1-bromo-benzene andits subsequent reaction with solid carbon dioxide (CO2) followed by acidic workup (using HCl asthe acid). "

Thus;

(A). C6H5Br + Mg(in ether) -----------> C6H5MgBr.

(B). C6H5MgBr + O = C = O -----------> C6H5-COO^- Mg^+ Br.

(C). C6H5-COO^- Mg^+ Br + HCl --------> C6H5-COOH + Mg^+Br(OH).

A student states that the graduated cylinder contains 150 mL of water his statement is
A. A prediction
B. An observation
C. A theory
D. A hypothesis

Answers

The correct answer is B. An observation

Explanation:

An observation is defined as a statement or conclusion you made after observing or measuring a phenomenon, this includes statements based on precise instruments. For example, if you conclude a plant grows 2 inches every month by measuring the plant during this time, this is classified as an observation. The conclusion of the student is also an observation because he concludes this after analyzing the volume of the water in the cylinder through the lines in the graduated cylinder, considering the water is just in the middle of 100 mL and 200 mL which indicates there are 150 mL of water.

Answer:

B. An observation

Explanation:

Hello,

Given the illustration, such statements is considered as an observation, since it came up from something the student realized with his/her own eyes, as in the volumetric cylinder the level of the liquid reached 150 mL of water. Predictions are not observed but assumed, theories are stated when experimentation is already deeply studied and hypothesis are assumptions before experimenting.

Regards.

The decomposition of Ca(OH)2(s) intoCaO(s) and H2O(g) at constant pressure requires the addition of 109 kJ of heat per mole of Ca(OH)2.
A. Write a balanced thermochemical equation for the reaction.
B. Draw an enthalpy diagram for the reaction, showing the activation energy, Ea, and the enthalpy change for the reaction.

Answers

Answer:

A. Ca(OH)2 ----> CaO + H2O; ∆H = +109KJ

B. Check attached document below for the enthalpy diagram

Explanation:

A thermochemical equation is a balanced chemical equation in which enthalpy change is variable. It tells about the nature of the reaction.

Enthalpy change is the difference between the heat content of the products and reactants in a thermochemical equation.

∆H is negative for an exothermic reaction (a reaction where heat is given out), while it is positive for an endothermic reaction ( a reaction in which heat is added).

The activation energy, Ea, is the minimum amount of energy reactant particles must possess in order for a reaction to proceed towards product formation.

As per the decomposition of the Ca(OH) 2 and the CaO the constant pressure needs to be added of the 109KJ.

The balance thermochemical equation for the reaction is expressed as  Ca(OH)2 ----> Ca O + H2O; ∆H = +109KJThe diagram for the reaction and the activation energy is given above.

Learn more about decomposition.

brainly.com/question/14797703.

Calculate the mass of CaCl2•2H2O required to make 100.0 mL of a 0.100 M solution. Each of the calculations below will take you through the necessary steps. You will be asked to show your answer and calculations for each. Calculate the moles of CaCl2•2H2O in 100.0 mL of a 0.100 M solution Enter your answer:

Answers

Answer:

The mass is 1.4701 grams and the moles is 0.01.

Explanation:

Based on the given question, the volume of the solution is 100 ml or 0.1 L and the molarity of the solution is 0.100 M. The moles of the solute (in the given case calcium chloride dihydride (CaCl2. H2O) can be determined by using the formula,  

Molarity = moles of solute/volume of solution in liters

Now putting the values we get,  

0.100 = moles of solute/0.1000

Moles of solute = 0.100 * 0.1000

= 0.01 moles

The mass of CaCl2.2H2O can be determined by using the formula,  

Moles = mass/molar mass

The molar mass of CaCl2.2H2O is 147.01 gram per mole. Now putting the values we get,  

0.01 = mass / 147.01

Mass = 147.01 * 0.01

= 1.4701 grams.  

The mass should be considered as the 1.4701 grams and the moles should be 0.01.

Calculation of the mass and moles:

Since we know that

Molarity = moles of solute/volume of solution in liters

So,

0.100 = moles of solute/0.1000

Moles of solute = 0.100 * 0.1000

= 0.01 moles

Now The mass should be

Moles = mass/molar mass

0.01 = mass / 147.01

Mass = 147.01 * 0.01

= 1.4701 grams.  

hence, The mass should be considered as the 1.4701 grams and the moles should be 0.01.

Learn more about moles here: https://brainly.com/question/24817060

How many grams of 02 are needed to react with 7.50g of ethanol

Answers

write eqn, find mols, compare ratio and take mols times mr of O2 to find mass

The calculated yield for the production of carbon dioxide was 73.4g. When the
experiment was performed in the lab, a yield of 72.3g was produced. What is the
percent yield of carbon dioxide?

Answers

Answer:10 grams of CO2

Explanation:

Yeild= exp. yeild÷ thoretical yeild × 100

Yeild= 73.3÷73.4 × 100

Yeild= 0.1 ×100

Yeild= 10

A student sets up the following equation to solve a problem in solution stoichiometry. (The ? stands for a number the student is going to calculate.) Enter the units of the student's answer

(1.26mol)1mL10^−3L / (7.9mol/L)= ?

Answers

Answer:

mL * L²

Explanation:

The question in t his problem is to calculate the units of the final answer.

The units in the numerator is mol, ml and L.

The unit in the denominator is mol/L

This leads us to;

Numerator / Denominator =  mol * mL * L / (mol / L )

The final units is mL * L²

Arrange the following compounds in order of increasing solubility in

water and explain your sequence.

C7H15OH C6H13OH C6H6 C2H5OH​

Answers

Answer:

C6H6<C7H15OH<C6H13OH<C2H5OH​

Explanation:

Organic substances are ordinarily nonpolar. This means that they do not dissolve in water. However, certain homologous series of organic compounds actually dissolve in water because they possess certain functional groups that effectively interact with water via hydrogen bonding.

A typical example of this is alcohol family. All members of this homologous series contain the -OH functional group. This group can effectively interact with water via hydrogen bonding, leading to the dissolution of low molecular weight alcohols in water.

Low molecular weight alcohols are miscible with water in all proportions. This implies that they are highly soluble in water. However, as the size of the alkyl moiety in the alcohol increases, the solubility of the alcohol in water decreases due to less effective interaction of the -OH group with water via hydrogen bonding. This explains the fact that C2H5OH​ is the most soluble alcohol in the list.

C6H6 is insoluble in water since it is purely a hydrocarbon with no -OH group capable of interaction with water via hydrogen bonding.

Hi I have a lab for Chemistry I am struggling with. I have to do calculations given the following information
1. Mass of evaporating dish plus sample 26.57 g
2. Mass of evaporating dish 24.29 g
3. Mass of evaporating plus NaCl 68.66 g
4. Mass of evaporating dish 67.84 g
5. Mass of filter paper plus sand 37.69 g
6. Mass of filter paper 36.34 g
CALCULATIONS AND CONCLUSIONS
1. Calculate the mass of unknown mixture g

2. Calculate the mass of NaCl recovered g

3. Calculate the mass of sand recovered g

4. Calculate the percentage of NaCl in your unknown mixture %

5. Calculate the percent sand in your unknown mixture %

6. Calculate the total mass of sand and salt recovered g

7. Calculate the percent recovery of the components %

Answers

Answer:

1.  2.28 g

2. 0.82 g

3. 1.35 g

4. 36 %

5. 59 %

6. 2.17 g

7. 95 %

Explanation:

Hello,

1. In this case, the mass of the unknown mixture is obtained by subtracting the mass of the dish plus sample and the mass of the dish:

m = 26.57 g- 24.29 g = 2.28 g

2. In this case, the mass of the NaCl recovered is obtained by subtracting the mass of the dish plus NaCl and the mass of the dish:

m = 68.66 g- 67.84 g = 0.82 g

3. In this case, the mass of the sand recovered is obtained by subtracting the mass of the filter paper plus sand and the mass of the filter paper:

m = 37.69 g- 36.34 g = 1.35 g

4. The percentage of NaCl is computed by considering its mass and the mass of the unknown mixture:

% NaCl = 0.82 g / 2.28 g * 100 % = 36 %

5. The percentage of sand is computed by considering its mass and the mass of the unknown mixture:

% sand = 1.35 g / 2.28 g * 100 % = 59 %

6. Here,we have to add the mass of NaCl and sand:

m = 0.82 g + 1.35 g = 2.17 g

7. Finally, the percent recovery is obtained by diving the total recovered mass by the total obtained mass of the mixture:

% recovery = 2.17 g / 2.28 g * 100 % = 95 %

Best regards.

what is a mitochondrion

Answers

Explanation:

Mitochondria (sing. mitochondria) are organelles, or parts of the eukaryote cell. They are in the cytoplasm, not the nucleus. They make the most cell supply of adenosine triphosphate (ATP), a molecule that cells use as an energy source. ... This means that mitochondria are known as '' the powerhouse of the cell'' or ''cell strength".

Good Luck, and have a great day..

an organelle found in large numbers in most cells, in which the biochemical processes of respiration and energy production occur. It has a double membrane, the inner layer being folded inward to form layers (cristae

2 FONS
How does the electric force between two charged particles change if the
distance between them is increased by a factor of 22
A. It increases by a factor of 4.
B. It increases by a factor of 2.
C. It decreases by a factor of 4
O
D. It decreases by a factor of 2.
SUB

Answers

Answer:

C. It decreases by a factor of 4

Explanation:

F1 = kq1*q2/r²

F2 = kq1*q2/(2r)² = kq1*q2/(4r²) = kq1*q2/(r²*4)  = F1/4

What allows two or more atoms to be held together?

Answers

Answer:

Atoms come together to form molecules because of their electrons. Electrons can join (or bond) atoms together in two main ways. When two atoms share electrons between them, they are locked together (bonded) by that sharing. These are called covalent bonds.

Explanation:

Answer:

Electrons

Explanation:

took the test got 100%

. The pI is called ________________. The rule of calculating pI of an amino acid is that first, write the dissociation equation from fully protonated form to fully deprotonated form, label the charge of each form; second, identify the zwitterionic form (zero charge) and find the closest pKs (left and right side in the dissociation equation); third, average these two pKs. Write the dissociation equations for amino acids, glutamate, histidine, and calculate their pIs.

Answers

Answer:

The isoelectric point is that the pH at which the compound is in an electronically neutral form.

For diss equations, please find them in the enclosed file.

The pIs of 2 amino acids:

Glutamate: pI = 3,2Histidine: pI = 7,6

Explanation:

Formula for the pI calculation: pI = (pKa1 + pKa2)/2

Given 3 pKa :

Acid glutamic with an acid sidechain:

Use the lower 2  pKas (corresponding with 2 -COOH groups)

pKa1 = 2,19; pKa2 = 4,25; so pI = 3,2

Histidine with 2 amino groups:

Use the higher 2 pKas ( -COOH group and -NH= group)

pKa1 = 6; pKa2 = 9,17; so pI = 7,6

What would cause a balloon to expand if taken to the top of a mountain?
O A. Increased molecular collision
O B. Increased amount of molecules
O C. Lowered temperature
D. Lowered pressure

Answers

Answer:

D. Lowered pressure

Explanation:

As you go to more altitude or height, the atmospheric pressure significantly lowers so the gas molecules are free to expand and take up as room as possible.

This is best explained by Boyle's law where pressure and volume are inversely related, where if one thing goes up another goes down. Here the pressure goes down, so volume increases and ballon expands.

Which of these scientists diagnosed smallpox and measles?

A. Nicolaus Copernicus

B. Al-Razi

C. Archimedes

D. Rosalind Franklin

Answers

......................B. Al-Razi

Answer:

B

Explanation:

What is in period 6 group 8

Answers

Answer:

Osmium

Explanation:

If you take a look at the attached image of a periodic table below, you will see that the element in the 6th period and 8th group is Osmium. Hope this helps!

An excess of AgNO3 reacts with 185.5 mL of an AlCl3 solution to give 0.325 g of AgCl. What is the concentration, in moles per liter, of the AlCl3 solution? Must show your work on scratch paper to receive credit. AlCl3(aq) + 3 AgNO3(aq) → 3 AgCl(s) + Al(NO3)3(aq)

Answers

Answer:

4.07x10⁻³M AlCl₃.

Explanation:

Based on the reaction:

AlCl₃(aq) + 3 AgNO₃(aq) → 3 AgCl(s) + Al(NO₃)₃(aq)

That means 1 mole of AlCl₃ reacts with 3 moles of AgNO₃ to produce 3 moles of AgCl.

As 0.325g of AgCl are produced. Moles of AgCl are (Molar mass AgCl: 143.32g/mol):

0.325g AgCl ₓ ( 1 mol / 143.32g) = 2.27x10⁻³ moles of AgCl

As 3 moles of AgCl are produced from 1 mole of AlCl₃, moles of AlCl₃ that produce 2.27x10⁻³ moles of AgCl are:

2.27x10⁻³ moles of AgCl ₓ (1 mole AlCl₃ / 3 moles AgCl) =

7.56x10⁻⁴ moles AlCl₃

As volume of the AlCl₃ solution that reacts is 185.5mL = 0.1855L, molar concentration of the solution is:

7.56x10⁻⁴ moles AlCl₃ / 0.1855L =

4.07x10⁻³M AlCl₃

Which of the following are not created by an arrangement of electric charges
or a current (the flow of electric charges)?
A. An electric field
B. A magnetic field
C. A quantum field
D. A gravitational field

Answers

Answer:

gravitational and quantum ARE NOT, but electric and magnetic ARE.    there is a similar question to this but it's the exact opposite, so don't get confused

Quantum number of boron

Answers

Answer:

The answer is 5.

symbol for carboxylic acid​

Answers

C(=O)OH The general formula of a carboxylic acid is R–COOH, with R referring to the alkyl group.

Which statement describes a chemical property of an object? A:The object is white in color.B:The object has a powdery texture.C:The object’s density is 2.11 g/cm3.D:The object reacts with acid to form water.

Answers

Answer:

D

Explanation:

Color, texture, and density are all physical properties but reactivity is a chemical property so the answer is D.

A gaseous system undergoes a change in temperature and volume. What is the entropy change for a particle in this system if the final number of microstates is 0.842 times that of the initial number of microstates

Answers

Answer: -2.373  x 10^-24J/K(particles

Explanation: Entropy is defined as the degree of randomness of a system which is a function of the state of a system and depends on the number of the random microstates present.

The entropy change for a particle in a system  depends on the initial and final states of a system and is given by Boltzmann equation as  

S = k ln(W) .

where S =Entropy

K IS Boltzmann constant ==1.38 x 10 ^-23J/K

W is the number of microstates available to the system.

 The  change in entropy is given as

S2 -S1 = kln W2 - klnW1

dS = k ln (W2/W1)

where w1 and w2 are initial and final microstates

from the question, W2(final) = 0.842 x W1(initial), so:

= 1.38*10-23 ln (0.842)

=1.38*10-23  x -0.1719

= -2.373  x 10^-24J/K(particles)

Methods in electrochemistry that can be used for the separation of proteins and enzymes?

Answers

Answer:

Some of the methods in Methods in electrochemistry that can be used for the separation of proteins and enzymes are as follows:

Redox transformations: In this method enzymes or proteins would be adsorbed on the electrode surface and facilitates direct electron transfer that causes denaturation and loss of their electrochemical activities and bioactivities. It is widely used in biosensors and biofuel cells.

Protein electrophoresis: In this process proteins are seperated by placing them in a gel matrix in the presence of an electrical field. In this method a negative charge is applied so that proteins move towards a positive charge.

When 25ml of sulphuric acid, was titrated with 0.0820 mol/L sodium hydroxide solution the end point was detected (with phenolphthalein) at 22.5ml . Calculate the concentration of sulphuric
acid in mol/L.​

Answers

Answer:

the concentration of sulphuric acid is 14mol/l

Other Questions
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